Organic chemistry instrumentala analysis

Research groups using the lab

The research groups that belong to the organic synthesis, photochemistry, environmental chemistry, polymeric materials, analytical sciences and supramolecular chemistry of the Department of Chemistry and the research groups of Pharmaceutical Chemistry of the Department of Pharmacy and Biotechnology access the laboratory and instrumentation.

Description

The laboratory performs qualitative and quantitative analysis for the characterization of compounds from organic synthesis, polymeric materials, study of compounds for electrochemical and photochemical applications. The present instrumentation allows the chromatographic separation, also in large scale, and the study of compounds also in complex matrices, by mass spectrometry and UV and IR spectroscopy.

Instrumentation

HPLC preparative Agilent Technologies 1100 series DAD UV-Vis

The instrument allows the large-scale separation and purification of organic synthesis products.

HPLC preparative Biotage

The instrument allows the large-scale separation and purification of organic synthesis products.

HPLC analitical Agilent Technologies 1100 series DAD UV-Vis interfaced with mass spectrometer ESI-APCI Ion-Trap Bruker-Agilent

The instrument allows the analytical separation of organic synthesis products and their characterization by mass spectrometer with Ion-Trap

HPLC analitical Agilent Technologies 1100 series DAD UV-Vis interfaced with mass spectrometer ESI-APCI single quadrupole

The instrument allows the analytical separation of organic synthesis products and their characterization by mass spectrometer with single quadrupole.

HPLC analitical Agilent Technologies 1200 Infinity II DAD UV-Vis interfaced with mass spectrometer ESI-APCI single quadrupole

The instrument allows the analytical separation of organic synthesis products and their characterization by mass spectrometer with single quadrupole.

HPLC analitical Waters Alliance 2695 DAD UV-Vis interfaced with mass spectrometer ESI triple quadrupole Quattro micro

The instrument allows the analytical separation of organic synthesis products and their characterization by mass spectrometer with triple quadrupole.

HPLC analitical Agilent Technologies 1200 series DAD UV-Vis

The instrument allows the analytical separation of organic synthesis products and is dedicated to the use of chiral columns for the determination of enantiomeric excesses.

GC Agilent Technologies 6850 interfaced with mass spectrometer single quadrupole MSD 5975

The instrument allows analytical chromatographic separation of organic synthesis products and their characterization by mass spectrometer with single quadrupole.

FT-IR Bruker Alpha System equipped with ATR Diamond system

The instrument allows spectroscopic analysis with IR technique both in transmittance and absolute total reflection.

Polarimeter SCHMIDT-HAENSCH Unipol L1000

The instrument allows the measurement of the rotational power of optically active products in solution.

GC Agilent Technologies 6890 series II detector FID

The instrument allows the gas chromatographic separation of organic synthesis products.

GC Agilent Technologies 5890 detector FID

The instrument allows the gas chromatographic separation of organic synthesis products.

Melting point measuring instruments

The laboratory contains various instruments for measuring the melting point of substances in the solid state

Consultancy

The instrumentation present in the instrumental laboratory of Organic Chemistry is also used for requests for analysis by external companies and in various consultancy and / or commissioned research contracts.

Teaching and training activity

All the instruments present in the instrumental laboratory of Organic Chemistry are used for the didactic activities of the laboratory courses of Organic Chemistry, Analytical Chemistry and Inorganic Chemistry for the three-year and master's degrees in Chemistry, Biology and Biotechnology. Furthermore, the same instrumentation is available to undergraduates and PhD students of organic synthesis groups and other groups of the "Ciamician" Department

Lab manager

Dr. Andrea Garelli, mobile: 335 68 62 614 Tel: 051-20 99589

Instruments

FT-IR Bruker

GC Agilent 5890

GC Agilent 6890

GC-MS Agilent

HPLC 1100 ion trap

HPLC 1100 single quadrupole

HPLC 1200

HPLC 1200 infinity single quadrupole

HPLC analytical

HPLC preparative 1100

HPLC preparative Biotage

Polarimeter Unipol 1000

Melting point